2-(4-溴苯氧基)-2-甲基丙酸乙酯合成路线 (共 3 条)
反应条件
thionyl chloride
T=20°C; 6 h; Heating / reflux;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; BOEHRINGER INGELHEIM PHARMA GMBH and CO. KG
Patent: WO2009/52078 A1, 2009 ;
Location in patent: Page/Page column 66 ;
WO 2009/052078 A1
反应条件
ethanol; sulfuric acid
参考文献
Julia
Bulletin de la Societe Chimique de France, 1956 , p. 776,780, 781
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=110°C;
参考文献
Yao, Wenqing; Xu, Meizhong; Zhang, Colin; Agrios, Konstantinos; Metcalf, Brian W.; Zhuo, Jincong
Patent: US2006/9471 A1, 2006 ;
Location in patent: Page/Page column 30-31 ;