反应条件
1: 1,3-diamino-propane With polymer-bound 4-chloro-3-hydroxymethylphenyldiazonium*BF4 in tetrahydrofuran
T=0°C; 0.5 h;
2: phenyl isocyanate in N,N-dimethyl-formamide
T=20°C; 2 h;
3: With trifluoroacetic acid in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Dahmen, Stefan; Brse, Stefan
Angewandte Chemie - International Edition, 2000 , vol. 39, # 20 p. 3681 - 3683