3,4,5-三甲氧基苯甲醛二甲基缩醛合成路线 （共 17 条）
反应条件
montmorillonite K10 in methanol T=40°C; 18 h; Inert atmosphere;
参考文献
Laurent, Mathieu Y.; Stocker, Vivien; Temgoua, Valery Momo; Dujardin, Gilles; Dhal, Robert
Tetrahedron Letters, 2011 , vol. 52, # 14 p. 1608 - 1611
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal T=20°C; P=760.051 Torr; 0.0833333 h;
参考文献
Tetrahedron, , vol. 63, # 38 p. 9382 - 9386
反应条件
hydrogenchloride 0.5 h;
参考文献
Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Zhu, Rui; Liu, Bo; Hu, Yuefei
Tetrahedron, 2007 , vol. 63, # 38 p. 9382 - 9386
反应条件
aluminum oxide; carbon dioxide; Isopulegol T=200°C; P=110207 Torr; Supercritical conditions;
参考文献
Russian Journal of Physical Chemistry A, , vol. 87, # 3 p. 382 - 387
Kinet. Katal., , vol. 87, # 3 p. 403 - 408,6
反应条件
potassium in tetrahydrofuran T=45°C; 24 h;
参考文献
Azzena, Ugo; Melloni, Giovanni; Piroddi, Anna Maria; Azara, Emanuela; Contini, Stefania; Fenude, Emma
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3101 - 3106
反应条件
1: With 15-crown-5; sodium in tetrahydrofuran T=-20°C; 18 h; 2: With water in tetrahydrofuran Further stages.;
参考文献
Azzena, Ugo; Dettori, Giovanna; Mascia, Ilaria; Pisano, Luisa; Pittalis, Mario
Tetrahedron, 2007 , vol. 63, # 48 p. 11998 - 12006
反应条件
trifluoroacetic acid in dichloromethane T=25°C; 16 h;
参考文献
Li, Wei; Li, Jianchang; Wu, Yuchuan; Fuller, Nathan; Markus, Michelle A.
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1077 - 1086
反应条件
1: With naphthalene; lithium in tetrahydrofuran T=-50°C; 16 h; 2: With water in tetrahydrofuran Further stages.;
参考文献
Azzena, Ugo; Dettori, Giovanna; Mascia, Ilaria; Pisano, Luisa; Pittalis, Mario
Tetrahedron, 2007 , vol. 63, # 48 p. 11998 - 12006
反应条件
2-iodo-propane; sodium
参考文献
Azzena, Ugo; Cossu, Sergio; Denurra, Teresa; Melloni, Giovanni; Piroddi, Anna Maria
Synthesis, 1990 , p. 313 - 314
反应条件
1: 1) Na / 1) THF, 24h, r.t., 2) THF, 3h, -40 deg C 2: AcOH / H2O / 5 h / Heating View Scheme
参考文献
Azzena, Ugo; Melloni, Giovanni; Piroddi, Anna Maria; Azara, Emanuela; Contini, Stefania; Fenude, Emma
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3101 - 3106
