2-[(乙酰氧基)甲氧基]乙基乙酸酯合成路线 （共 38 条）
反应条件
CsI in acetonitrile 12 h; Heating; Yield given. Yields of byproduct given;
参考文献
Kim, Yong Hae; Kim, Joong Young; Lee, Chun Ho
Chemistry Letters, 1988 , p. 1045 - 1048
反应条件
ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane in water; acetone
参考文献
Syntex (U.S.A.) Inc.
Patent: US5565565 A1, 1996 ;
反应条件
CsI in acetonitrile 3 h; Heating;
参考文献
Kim, Yong Hae; Kim, Joong Young; Lee, Chun Ho
Chemistry Letters, 1988 , p. 1045 - 1048
反应条件
CsI in acetonitrile 12 h; Heating; Yield given. Yields of byproduct given;
参考文献
Kim, Yong Hae; Kim, Joong Young; Lee, Chun Ho
Chemistry Letters, 1988 , p. 1045 - 1048
反应条件
ammonium sulfate; CsI multistep reaction; also with other purine and pyrimidine bases; catalysts tested: CsBr, CsCl, CsF; Product distribution;
参考文献
Kim, Yong Hae; Kim, Joong Young; Lee, Chun Ho
Chemistry Letters, 1988 , p. 1045 - 1048
反应条件
1: 2.) p-toluenesulfonic acid monohydrate / 1.) acetic acid, 140 deg C, 18 h, 2.) DMSO, 100 deg C, 16 h 2: 81 percent / 28 percent sodium methylate, methanol / 16 h / Ambient temperature View Scheme
参考文献
Matsumoto; Kaneko; Yamada; Takeuchi; Mori; Mizuno
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 3 p. 1153 - 1157
反应条件
toluene-4-sulfonic acid in chlorobenzene; acetonitrile T=120°C; 2 h;
参考文献
Boryski, Jerzy
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 3 p. 649 - 652
反应条件
chloro-trimethyl-silane; tin(IV) chloride; 1,1,1,3,3,3-hexamethyl-disilazane
1.) reflux, 3 h, 2.) a) RT, 18 h, b) reflux, 5 d; Yield given. Multistep reaction;
参考文献
Kelley, James L.; Kelsey, John E.; Hall, William R.; Krochmal, Mark P.; Schaeffer, Howard J.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 6 p. 753 - 756
反应条件
ammonium sulfate; CsI
2.) acetonitrile, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Kim, Yong Hae; Kim, Joong Young; Lee, Chun Ho
Chemistry Letters, 1988 , p. 1045 - 1048
反应条件
tin(IV) chloride
1.) CH2Cl2, RT, 3 h, 2.) CH2Cl2, RT, overnight; Yield given. Multistep reaction;
参考文献
Rosowsky; Kim; Wick
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1177 - 1181
