2-[(乙酰氧基)甲氧基]乙基乙酸酯合成路线 （共 38 条）
反应条件
tin(IV) chloride
1.) CH2Cl2, RT, overnight, 2.) CH2Cl2, 25 deg C, overnight; Yield given. Multistep reaction;
参考文献
Rosowsky; Kim; Wick
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1177 - 1181
反应条件
ammonium sulfate; chlorosulphonyl isocyanate in acetonitrile
2 h; Heating;
参考文献
Ubasawa, Masaru; Takashima, Hideaki; Sekiya, Kouichi
Nucleosides and Nucleotides, 1998 , vol. 17, # 12 p. 2241 - 2247
反应条件
N,O-bis-(trimethylsilyl)-acetamide in dichloromethane
参考文献
University of North Carolina; Macronex, Inc.
Patent: US5550132 A1, 1996 ;
反应条件
aluminum oxide; silica gel
0.0666667 h; microwave irradiation;
参考文献
Qu, Guirong; Han, Suhui; Zhang, Zhiguang; Geng, Mingwei; Xue, Feng
Canadian Journal of Chemistry, 2006 , vol. 84, # 5 p. 819 - 824
反应条件
0.166667 h; microwave irradiation;
参考文献
Qu, Guirong; Han, Suhui; Zhang, Zhiguang; Geng, Mingwei; Xue, Feng
Canadian Journal of Chemistry, 2006 , vol. 84, # 5 p. 819 - 824
反应条件
sodium hydroxide; toluene-4-sulfonic acid
1.) 100 deg C, 20 h, 2.) room temperature, overnight; Yield given. Multistep reaction;
参考文献
Shiragami; Koguchi; Tanaka; Takamatsu; Uchida; Ineyama; Izawa
Nucleosides and Nucleotides, 1995 , vol. 14, # 3-5 p. 337 - 340
反应条件
in chloroform; benzene
参考文献
Burroughs Wellcome Co.
Patent: US4146715 A1, 1979 ;
反应条件
aluminum oxide; silica gel
0.1 h; microwave irradiation;
参考文献
Qu, Guirong; Han, Suhui; Zhang, Zhiguang; Geng, Mingwei; Xue, Feng
Canadian Journal of Chemistry, 2006 , vol. 84, # 5 p. 819 - 824
