N-叔丁氧羰基-L-谷氨酸二甲酯合成路线 （共 26 条）
反应条件
1: pyridine / 12 h / 20 °C 2: 85.4 percent / DMAP / acetonitrile / 20 °C 3: lithium bromide / acetonitrile / 10 h / 65 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 3 p. 743 - 746
反应条件
1: 85.4 percent / DMAP / acetonitrile / 20 °C 2: lithium bromide / acetonitrile / 10 h / 65 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 3 p. 743 - 746
参考文献
Carbohydrate Research, , vol. 47, p. 49 - 61
反应条件
1: aq. NaOH / dioxane / 20 °C 2: diethyl ether / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 43 p. 7599 - 7603
反应条件
1: NaOH; H2O / tetrahydrofuran / 5 h / 20 °C 2: K2CO3 / dimethylformamide / 6 h / 20 °C 3: 43 percent / Br2; NaOMe / 0.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 15 p. 2057 - 2060
反应条件
1: K2CO3 / dimethylformamide / 6 h / 20 °C 2: 43 percent / Br2; NaOMe / 0.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 15 p. 2057 - 2060
反应条件
bromine; sodium methylate Substitution; 0.5 h; Heating;
参考文献
Matsumura, Yoshihiro; Yuki Satoh, Kimihiro Shirai; Onomura, Osamu; Toshihide, Maki
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 15 p. 2057 - 2060
反应条件
1: 98 percent / DMAP / acetonitrile / Ambient temperature 2: 85 percent / DIBAL / diethyl ether; hexane / 0.08 h / -78 °C View Scheme
参考文献
Wu, Wenbin; Li, Zheng; Zhou, Guangbiao; Jiang, Sheng
Tetrahedron Letters, 2011 , vol. 52, # 19 p. 2488 - 2491
反应条件
1: NaBH4, CaCl2 / ethanol / 2 h / 0 °C 2: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 3: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme
参考文献
Moon, Sung-Hwan; Lee, Sujin
Synthetic Communications, 1998 , vol. 28, # 21 p. 3919 - 3926
反应条件
1: 31 percent / lithium diisopropylamide / tetrahydrofuran; hexane / -78 - -20 °C 2: 91 percent / NH2OH*HCl / H2O; dioxane / 1 h / Ambient temperature 3: 75 percent / 2N NaOH / methanol / 2 h / Ambient temperature 4: 87 percent / 2N NaOH / methanol / 2 h / Ambient temperature 5: trifluoroacetic acid / 30 h / Ambient temperature View Scheme
参考文献
Tsubotani, Shigetoshi; Funabashi, Yasunori; Takamoto, Masayuki; Hakoda, Seiji; Harada, Setsuo
Tetrahedron, 1991 , vol. 47, # 38 p. 8079 - 8090
