反应条件
1: 1.) LDA / 1.) hexane, THF, -78 deg C, 30 min, 2.) hexane, THF, from -78 to 10 deg C
2: m-chloroperoxybenzoic acid / hexane / 4 h / Ambient temperature
View Scheme
参考文献
White, Andrew D.; Creswell, Mark W.; Chucholowski, Alexander W.; Blankley, C. John; Wilson, Michael W.; Bousley, Richard F.; Essenburg, Arnold D.; Hamelehle, Katherine L.; Krause, Brian R.; Stanfield, Richard L.; Dominick, Mark A.; Neub, Martin
Journal of Medicinal Chemistry, 1996 , vol. 39, # 22 p. 4382 - 4395