反应条件
1: 45.2 percent / MeONa / methanol / 35 °C / electrolysis on Pt electrode, 0.05 amps, 50-60 volts 2: KOH 3: 48.6 percent / MeONa / methanol / 35 °C / electrolysis on Pt electrode, 0.05 amps, 50-60 volts 4: 96 percent / LiAlH4 / tetrahydrofuran / 1.) -10 deg C -> room temperature, 1 h, 2.) room temperature, 4 h View Scheme
参考文献
Synthetic Communications, , vol. 14, # 7 p. 681 - 686
