反应条件
in methanol Schlenk techniques or gloveboxes under Ar used, trans-(hfac-O,O)2Rh(Cl)(CH3OH) (apprx. 1.0 g) dissolved in MeOH, Me2Hg added (2:1 molar ratio), heated for 14 h at 75 °C; excess Me2Hg and MeOH removed in vac., redissolved in minimal volume of MeOH, kept at -30 °C, filtered, solvent removed under vac.; NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 696, # 2 p. 551 - 558
