lithium borohydride in diethyl ether T=-78 - 20°C;
参考文献
Aldridge, Simon; Downs, Anthony J.; Tang, Christina Y.; Parsons, Simon; Clarke, Michael C.; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 2231 - 2243
in diethyl ether byproducts: H2; stirring at room temp. until end of H2-evolution, boiling for 1h, filtration, evapn.;;
参考文献
Schaeffer, G. W.; Anderson, E. B.
Journal of the American Chemical Society, 1949 , vol. 71, p. 2143 - 2145
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
