in water byproducts: H2; slow addn. of H2O to a mixture of NaBH4 and ((CH3)3NH)Cl in N(CH3)3 at -10°C while stirring (3h), addn. of H2O and petroleum ether, evapn. of petroleum ether phase;;
参考文献
Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
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U. S. Borax & Chemical Corp.
Patent: GB952811 , 1964 ;
C. A., 1964 , vol. 61, p. 2970
in benzene under N2 or Ar mixt. in stoich. quantity stirred at room temp. for 2 h; volatile components removed by vac. distn., crude product sublimed at 32°C; elem. anal.;
Vincent
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1877 , vol. 84, p. 1139
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1877 , vol. 85, p. 667
