in neat (no solvent) (exclusion of moisture); room temp., 16 h; purifn. by trap-to-trap distn.;
参考文献
Aldridge, Simon; Blake, Alexander J.; Downs, Anthony J.; Parsons, Simon; Pulham, Colin R.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 853 - 859
in benzene-d6 under Ar; in NMR tube; Al complex and B(C6F5)3 (molar ratio 3:1) dissolved in benzene-d6; stirred at room temp. for 12 h; not isolated; monitored by NMR spectra;
Naturforschung und Medizin in Deutschland 1939-1946, fuer Deutschland bestimmte Ausgabe der FIAT Review of German Science, Dieterichsche Verlagsbuchhandlung, Wiesbaden. Bd. 23, S. 226
in deuterated toluene not isolated, identified by NMR;
参考文献
Organometallics, , vol. 20, # 17 p. 3772 - 3776
→
反应条件
in chloroform-d1 N2; 60 min at room temp.; boron NMR data indicated presence of BMe3 and B5H9 only, the products, expected from the decompn. of BMe2B5H8;
参考文献
Saulys, D. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 4174 - 4179
