4-三甲硅基-3-丁炔-2-酮合成路线 （共 32 条）
反应条件
sodium carbonate in acetonitrile T=120°C; 0.666667 h; microwave irradiation;
参考文献
Bagley, Mark C.; Hughes, David D.; Taylor, Paul H.
Synlett, 2003 , # 2 p. 259 - 261
反应条件
anhydrous sodium borate; water
参考文献
Heiss, Christian; Phillips, Robert S.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2821 - 2825
反应条件
zinc dibromide in dimethyl sulfoxide T=110°C; Bohlmann-Rahtz heteroannulation; 72 h;
参考文献
Hughes, David D.; Bagley, Mark C.
Synlett, 2002 , # 8 p. 1332 - 1334
反应条件
sodium carbonate in acetonitrile T=120°C; 0.666667 h; microwave irradiation;
参考文献
Bagley, Mark C.; Hughes, David D.; Taylor, Paul H.
Synlett, 2003 , # 2 p. 259 - 261
参考文献
Shostakovskii,M.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1968 , vol. 38, p. 1172 - 1176,1126 - 1129
反应条件
ammonium acetate; [Hmim]CF3COO T=20°C; Bohlmann-Rahtz pyridine synthesis; 24 h;
参考文献
Karthikeyan, Ganesan; Perumal, Paramasivan T.
Canadian Journal of Chemistry, 2005 , vol. 83, # 10 p. 1746 - 1751
反应条件
ammonium acetate in ethanol Bohlmann-Rahtz reaction; 24 h; Heating;
参考文献
Xiong, Xin; Bagley, Mark C.; Chapaneri, Krishna
Tetrahedron Letters, 2004 , vol. 45, # 32 p. 6121 - 6124
反应条件
in dimethyl sulfoxide T=170°C; Bohlmann-Rahtz synthesis; 0.333333 h; microwave irradiation;
参考文献
Bagley, Mark C; Lunn, Rebecca; Xiong, Xin
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8331 - 8334
反应条件
ammonium acetate; zinc dibromide in toluene Bohlmann-Rahtz reaction; 20 h; Heating;
参考文献
Bagley, Mark C.; Dale, James W.; Bower, Justin
Chemical Communications, 2002 , # 16 p. 1682 - 1683
反应条件
1: tri-phenyl-antimony With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 4-(trimethylsilyl)-3-butyn-2-one With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
