N-甲基-N-苄基氨基甲酸乙酯合成路线 （共 10 条）
反应条件
sodium in xylene 9 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 52, # 16 p. 3699 - 3701
反应条件
1: benzyl-methyl-amine With N(Et)4ClO4 in acetonitrile
T=20°C; Electrochemical reactiondivided cells, Pt anode;
2: carbon dioxide in acetonitrile
T=20°C; 1 h;
3: ethyl iodide in acetonitrile
T=20°C; Further stages.;
参考文献
Feroci, Marta; Casadei, Maria Antonietta; Orsini, Monica; Palombi, Laura; Inesi, Achille
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1548 - 1551
反应条件
acetic acid in ethyl acetate; N,N-dimethyl-formamide; mineral oil
参考文献
MERCK and CO. INC.
Patent: EP486280 A2, 1992 ;
EP 0486280 A2
反应条件
in dichloromethane
T=20°C; 0.166667 h;
参考文献
Kita, Yasuyuki; Haruta, Jun-ichi; Tagawa, Hiroko; Tamura, Yasumitsu
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4519 - 4522
参考文献
Kita, Yasuyuki; Haruta, Jun-ichi; Tagawa, Hiroko; Tamura, Yasumitsu
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4519 - 4522
反应条件
MCM-41-TBD; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine
15 h; Heating;
参考文献
Carloni, Silvia; De Vos, Dirk E.; Jacobs, Pierre A.; Maggi, Raimondo; Sartori, Giovanni; Sartorio, Raffaella
Journal of Catalysis, 2002 , vol. 205, # 1 p. 199 - 204
反应条件
sodium hydride; N,N-dimethyl-formamide
参考文献
Dannley; Lukin
Journal of Organic Chemistry, 1957 , vol. 22, p. 268
反应条件
sodium hydride; N,N-dimethyl-formamide
参考文献
Dannley; Lukin
Journal of Organic Chemistry, 1957 , vol. 22, p. 268
反应条件
tetra-(n-butyl)ammonium iodide
1) electrolysis, cathode: 25-cm2-Hg, anode: C, DMF, 2h; Yield given. Multistep reaction;
参考文献
Hess, Ulrich; Dunkel, Silke
Zeitschrift fuer Chemie (Stuttgart, Germany), 1988 , vol. 28, # 10 p. 372 - 373
反应条件
1.) MeCN, rt, 1 h, 2.) MeCN, rt, overnight; Yield given. Multistep reaction;
参考文献
Inesi; Mucciante; Rossi
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1337 - 1338
