反式-3-(三甲基硅基)烯丙醇合成路线 （共 28 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Wilson, Stephen R.; Zucker, Paul A.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4682 - 4693
反应条件
sulfuric acid in hexane; ethyl acetate; toluene
参考文献
Merrell Dow Pharmaceuticals, Inc.
Patent: US5252587 A1, 1993 ;
反应条件
diisobutylaluminium hydride in dichloromethane; cyclohexane T=-78°C; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 4 p. 568 - 570
反应条件
lithium aluminium tetrahydride
参考文献
Yoshida, Jun-ichi; Maekawa, Tsuyoshi; Morita, Yuko; Isoe, Sachihiko
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1321 - 1322
反应条件
in diethyl ether 3 h; Ambient temperature;
参考文献
Altnau, G.; Roesch, L.; Bohlmann, F.; Lonitz, M.
Tetrahedron Letters, 1980 , vol. 21, p. 4069 - 4072
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Tetrahedron, , vol. 42, # 16 p. 4427 - 4436
反应条件
1: 100 percent / p-toluenesulfonic acid / methanol / Ambient temperature 2: 93 percent / Red-Al / toluene / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 52, # 21 p. 7487 - 7510
反应条件
1: 98 percent / meta-chloroperbenzoic acid / CH2Cl2 / 1 h / -70 °C 2: methyllithium / tetrahydrofuran; diethyl ether / 0.33 h / -70 °C 3: tetrahydrofuran; diethyl ether / 0.75 h / -70 °C 4: CCl4 / 0.33 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 23 p. 2371 - 2374
反应条件
1: methyllithium / tetrahydrofuran; diethyl ether / 0.33 h / -70 °C 2: tetrahydrofuran; diethyl ether / 0.75 h / -70 °C 3: CCl4 / 0.33 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 23 p. 2371 - 2374
反应条件
1: AlCl3 / CH2Cl2 / -40 °C 2: LiAlH4 View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2143 - 2146
