反式-3-(三甲基硅基)烯丙醇合成路线 （共 28 条）
反应条件
hydrogenchloride; chloro-(2-methylpropyl)magnesium; bis(cyclopentadienyl)titanium dichloride 1) ether, 25 deg C, 10 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1126 - 1127
反应条件
n-butyllithium; fluorodimethoxyborane*Et2O; potassium tert-butylate; dihydrogen peroxide 1.) THF, -50 deg C, 1 h; -75 deg C to 25 deg C, 2.) THF, 25 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 707 - 709
反应条件
trimethylaluminum; diisobutylaluminium hydride 1.) CH2Cl2, 2.) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 38, # 22 p. 3829 - 3832
反应条件
lithium aluminium tetrahydride
参考文献
Bulletin de la Societe Chimique de France, , p. 2143 - 2146
参考文献
Journal of Organic Chemistry, , vol. 62, # 3 p. 636 - 640
反应条件
1: 82 percent / Pyridine / tetrahydrofuran / 0 °C 2: 1.) Zn / THF, HMPA 3: 2.) H2O, H(1+) / 2.) heating View Scheme
参考文献
Wada, Makoto; Shigehisa, Takahide; Akiba, Kin-ya
Tetrahedron Letters, 1985 , vol. 26, # 42 p. 5191 - 5194
反应条件
triethylamine in dichloromethane
参考文献
Makino, Tatsuya; Itoh, Kenji
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 395 - 405
参考文献
Lesur, Brigitte; Ducep, Jean-Bernard; Lalloz, Marie-Noelle; Ehrhard, Anne; Danzin, Charles
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 3 p. 355 - 360
反应条件
manganese(IV) oxide in dichloromethane T=35°C; 8 h;
参考文献
Ostwald, Roswitha; Chavant, Pierre-Yves; Stadtmueller, Heinz; Knochel, Paul
Journal of Organic Chemistry, 1994 , vol. 59, # 15 p. 4143 - 4153
反应条件
propionic acid in toluene Heating;
参考文献
Stamos, Dean P.; Kishi, Yoshito
Tetrahedron Letters, 1996 , vol. 37, # 48 p. 8643 - 8646
