4-(4-甲氧基苯基)吡啶合成路线 （共 33 条）
反应条件
1.1: ZnCl2; CoCl2; Bu4NBF4 / acetonitrile; dimethylformamide / Electrochemical reaction 1.2: CuCN; LiCl / 2 h / 0 - 20 °C 2.1: SiO2; O2 / CH2Cl2 / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 57, # 10 p. 1923 - 1927
反应条件
1.1: ZnCl2; CoCl2; Bu4NBF4 / acetonitrile; dimethylformamide / Electrochemical reaction 1.2: CuCN; LiCl / 2 h / 0 - 20 °C 2.1: SiO2; O2 / CH2Cl2 / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 57, # 10 p. 1923 - 1927
反应条件
1.1: sodium hydroxide / water; toluene / 0.33 h / 0 - 5 °C / pH Ca. 9 2.1: magnesium; iodine / tetrahydrofuran / 3 h / 35 °C / |Inert atmosphere 2.2: 4.25 h / 30 - 45 °C / |Inert atmosphere View Scheme
参考文献
Organic Process Research and Development, , vol. 7, # 3 p. 436 - 445
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane; acetic acid T=80°C; 32 h;
参考文献
Tetrahedron, , vol. 60, # 29 p. 6217 - 6224
反应条件
hydrogenchloride; sodium nitrite 1.) H2O, 2.) H2O, 40 deg C, 2 h, 80 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 5 p. 1780 - 1789
反应条件
1: chloroform; aqueous hydrogen peroxide; aq. NaOH solution 2: 100 - 110 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 2213,2216
反应条件
potassium permanganate; copper(l) iodide 1.) THF, - 30 deg C, 1 h, 2.) Me2CO, 0 deg C,; Yield given. Multistep reaction;
参考文献
Angewandte Chemie, , vol. 104, # 11 p. 1554 - 1556
反应条件
hydrogenchloride; water
参考文献
Journal of the Chemical Society, , p. 358,359
反应条件
1: 4-methoxy-aniline With tetrafluoroboric acid; sodium nitrite in water T=0°C; Inert atmosphere; 2: pyridine hydrochloride With [Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in water T=25°C; 80 h; IrradiationInert atmosphere; Catalytic behavior; Reagent/catalyst;
参考文献
Chemistry - A European Journal, , vol. 20, # 10 p. 2960 - 2965
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 30, # 26 p. 3433 - 3436
