2-甲基-3-硝基苯甲酸乙酯合成路线 (共 3 条)
反应条件
1: N,N-dimethyl-formamide / 16 h / Inert atmosphere; Reflux 2: iron; acetic acid / ethanol / 0.5 h / 50 °C / Reflux; Inert atmosphere View Scheme
参考文献
Griffiths-Jones, Charlotte M.; Knight, David W.
Tetrahedron, 2011 , vol. 67, # 44 p. 8515 - 8528
反应条件
1: N,N-dimethyl-formamide / 16 h / Inert atmosphere; Reflux 2: iron; acetic acid / ethanol / 0.5 h / 50 °C / Reflux; Inert atmosphere 3: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether; toluene / 16 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Tetrahedron, , vol. 67, # 44 p. 8515 - 8528
反应条件
sulfuric acid
T=20°C; 168 h;
参考文献
Bhuiyan, M. Delower H.; Zhu, Kai-Xian; Jensen, Paul; Try, Andrew C.
European Journal of Organic Chemistry, 2010 , # 24 p. 4662 - 4670