(2-苯基-4-噁唑)-甲醇合成路线 (共 12 条)
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
1: PBr5 / benzene 2: methanol / Heating View Scheme
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
1) 3 h, -78 deg C, 2) to r.t.;
参考文献
Yoo, Sang-Ku
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2159 - 2162
反应条件
methanesulfonic acid; carbonic acid dimethyl ester
T=120°C; 1.33333 h; Microwave irradiation;
参考文献
Orr, David; Tolfrey, Alexandra; Percy, Jonathan M.; Frieman, Joanna; Harrison, Zoe A.; Campbell-Crawford, Matthew; Patel, Vipulkumar K.
Chemistry - A European Journal, 2013 , vol. 19, # 29 p. 9655 - 9662
反应条件
methanol; lithium borohydride in tetrahydrofuran
参考文献
Zylstra, Eric J.; She, Miles W.-L.; Salamant, Walter A.; Leahy, James W.
Synlett, 2007 , # 4 p. 623 - 627
反应条件
1: K2CO3 / methanol; H2O
2: lithium borohydride; MeOH / tetrahydrofuran
View Scheme
参考文献
Zylstra, Eric J.; She, Miles W.-L.; Salamant, Walter A.; Leahy, James W.
Synlett, 2007 , # 4 p. 623 - 627
反应条件
1: PPh3; CCl4; i-Pr2NEt / acetonitrile; CH2Cl2 / 0 - 20 °C
2: CuBr; DBU; HMTA / CH2Cl2
3: K2CO3 / methanol; H2O
4: lithium borohydride; MeOH / tetrahydrofuran
View Scheme
参考文献
Zylstra, Eric J.; She, Miles W.-L.; Salamant, Walter A.; Leahy, James W.
Synlett, 2007 , # 4 p. 623 - 627
反应条件
1: CuBr; DBU; HMTA / CH2Cl2
2: K2CO3 / methanol; H2O
3: lithium borohydride; MeOH / tetrahydrofuran
View Scheme
参考文献
Zylstra, Eric J.; She, Miles W.-L.; Salamant, Walter A.; Leahy, James W.
Synlett, 2007 , # 4 p. 623 - 627
反应条件
sodium tetrahydroborate in 1,4-dioxane
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411