in dichloromethane; toluene anhyd. MnI2 was stirred with an equimolar amount of PMe3 in toluene-CH2Cl2; solvents were removed under vac., residue was washed with toluene; elem. anal.;
参考文献
Beagley, Brian; McAuliffe, Charles A.; Minten, Karl; Pritchard, Robin G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 1999 - 2004
in toluene a soln. of trimethylphosphane is dropped to a suspension of (C8H14B)2Se2 in toluene, stirring at room temp. for 2 h, removing of the solvent, sublimation of SePMe3 at 60-80°C/0.001 Torr and of (C8H14B)2Se(PMe3) at 110-120°C/0.001 Torr;
