反应条件
in dichloromethane
V- and Fe-complexes were dissolved in CH2Cl2 with stirring, stirred for 15 min, cooled to -78°C, PMe3 was transferred, warmed to room temp. under N2; volatiles were removed in vacuo, washed with pentane, dried in vacuo, redissolved in CH2Cl2, filtered, pentane was added, dried in vacuo; elem. anal.;
参考文献
Brunker, Tim J.; Cowley, Andrew R.; O'Hare, Dermot
Organometallics, 2002 , vol. 21, # 15 p. 3123 - 3138
