反应条件
Na in ammonia; pentane
NH3 (liquid); Na reacted with trimethylchlorostannane in pentane/liq. NH3 under N2, 2,2-dichloropropane added slowly with stirring, NH3 allowed to boil off; extd. with pentane and H2O, pentane layer washed with H2O, evapd. (vac.), treated with H2O2/acetone, stirred, treated with pentane, washed withH2O, pentane layer dried (MgSO4), filtered, concd., distd. (0.01 Torr) at room temp.; elem. anal.;
参考文献
Karol, Thomas J.; Hutchinson, John P.; Hyde, Jeffrey R.; Kuivila, Henry G.; Zubieta, Jon A.
Organometallics, 1983 , vol. 2, p. 106 - 114
