反应条件
in tetrahydrofuran argon, added at -78°C, stirred at this temp. for 5 min, mixt was transfered to a soln. of water in THF, warmed to 25°C; solvent removed under vacuum, extracted with pentane, removal of the solvent, resulting oil was purified by glpc, elem. anal.;
参考文献
Organometallics, , vol. 10, p. 2424 - 2431
