in tetrahydrofuran exclusion of moisture, refluxed for 4 h; cooled, removal of solvent in vac., sublimation at 80°C (CH3ReO3); elem. anal., residue dissolved in THF, filtered, removal of solvent from the filtrate: ((CH3)3SnO)ReO3; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 372, p. 351 - 370
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; lithium chloride in various solvent(s) T=60°C; 48 h; other alkyltin compounds; var. phosphines and arsines; Rate constantProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 113, # 25 p. 9585 - 9595
