1-氯-4-[(氯甲基)磺酰基]苯合成路线 （共 14 条）
反应条件
in dimethyl sulfoxide
T=58°C; 12 h;
参考文献
Crozet, Maxime D.; Botta, Celine; Gasquet, Monique; Curti, Christophe; Remusat, Vincent; Hutter, Sebastien; Chapelle, Olivier; Azas, Nadine; De Meo, Michel; Vanelle, Patrice
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 2 p. 653 - 659
参考文献
Boehme; Fischer; Frank
Justus Liebigs Annalen der Chemie, 1949 , vol. 563, p. 54,64
反应条件
hydrogenchloride in diethyl ether
参考文献
van Leusen,A.M.; Strating,J.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 151 - 164
反应条件
1: NOCl, Py
2: diethyl ether
3: HCl / diethyl ether
View Scheme
参考文献
van Leusen,A.M.; Strating,J.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 151 - 164
反应条件
1: diethyl ether
2: HCl / diethyl ether
View Scheme
参考文献
van Leusen,A.M.; Strating,J.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 151 - 164
反应条件
1: sodium hydroxide / 170 - 190 °C
2: thionyl chloride
3: chromium (VI)-oxide; acetic acid
View Scheme
参考文献
Barber et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 266,273
Journal of Applied Chemistry, 1954 , vol. 4, p. 110,111
反应条件
hydrogenchloride
Diazotization.Kochen der Diazoniumsalz-Loesung mit CuCl;
参考文献
Jain; Iyer; Guha
Journal of the Indian Chemical Society, 1947 , vol. 24, p. 220
反应条件
1: thionyl chloride
2: chromium (VI)-oxide; acetic acid
View Scheme
参考文献
Barber et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 266,273
Journal of Applied Chemistry, 1954 , vol. 4, p. 110,111
反应条件
1: aq. NaOH solution
2: aqueous hydrochloric acid
3: aqueous HCl / Diazotization.Kochen der Diazoniumsalz-Loesung mit CuCl
View Scheme
参考文献
Jain; Iyer; Guha
Journal of the Indian Chemical Society, 1947 , vol. 24, p. 220
反应条件
1: aqueous hydrochloric acid
2: aqueous HCl / Diazotization.Kochen der Diazoniumsalz-Loesung mit CuCl
View Scheme
参考文献
Jain; Iyer; Guha
Journal of the Indian Chemical Society, 1947 , vol. 24, p. 220
