反应条件
in dichloromethane Schlenk techniques under N2 used, HSnPh3 (0.194 mmol) added to CH2Cl2 soln. of IrCl(CO)(PPh3)2 (0.038 mmol), stirred for 7 h; solvent removed in vac., washed with hexane, redissolved in CH2Cl2, filtered, concd., hexane added, allowed to stay at -20°C for 30 min, ppt. collected, washed with hexane; XRD;
参考文献
Journal of Organometallic Chemistry, , vol. 696, # 17 p. 2904 - 2909
