反应条件
pyridine; sodium methylate; triethylamine 1.) AcOH, 5-7 deg C, 8 h, constant current electrolysis (Pt, 240 mA, 30-50 V); 2.) MeOH, 24 deg C, 30 min; 3.) 35 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 10 p. 3078 - 3086