1,3-二棕榈酰-2-磷脂酰胆碱合成路线 （共 5 条）
反应条件
1.1: pyridine / diethyl ether / 20 °C
1.2: H2O / 1 h
2.1: CHCl3; acetonitrile; propan-2-ol / 50 °C
View Scheme
参考文献
Haftendorn, Regine; Schwarze, Gabriele; Ulbrich-Hofmann, Renate
Chemistry and Physics of Lipids, 2000 , vol. 104, # 1 p. 57 - 66
反应条件
in chloroform; water; isopropyl alcohol; acetonitrile
36 h;
参考文献
Zaffalon, Pierre-Leonard; Zumbuehl, Andreas
Synthesis, 2011 , # 5 p. 778 - 782
反应条件
1: trifluoroacetic acid / dichloromethane / 36 h
2: chloroform; water; isopropyl alcohol; acetonitrile / 36 h
View Scheme
参考文献
Zaffalon, Pierre-Leonard; Zumbuehl, Andreas
Synthesis, 2011 , # 5 p. 778 - 782
反应条件
1: pyridine / tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 6.5 h / 0 °C
3: tetrahydrofuran / 0 °C
4: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 1 h / 0 - 20 °C
5: trifluoroacetic acid / dichloromethane / 36 h
6: chloroform; water; isopropyl alcohol; acetonitrile / 36 h
View Scheme
参考文献
Zaffalon, Pierre-Leonard; Zumbuehl, Andreas
Synthesis, 2011 , # 5 p. 778 - 782
反应条件
pyridine; chloroform
参考文献
Obata
Rikagaku Kenkyusho Iho, 1943 , vol. 22, p. 117
Chem.Abstr., 1948 , p. 522
