1-溴-4-(二甲基氨基)萘合成路线 （共 6 条）
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one in dichloromethane T=-10 - 20°C;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 2 p. 297 - 303
反应条件
potassium carbonate in N,N-dimethyl-formamide 1.) 65 deg C, 25 h, 2.) 120 Deg C, 3 h; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 13 p. 4051 - 4066
参考文献
Journal of the American Chemical Society, , vol. 70, p. 234,236
反应条件
sodium hydroxide 1) 180 deg C, 5 h; 2) reflux, 1.5 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 2 p. 297 - 303
反应条件
n-butyllithium; diethyl ether Behandeln des Reaktionsprodukts mit CO2;
参考文献
Fischer et al.
Journal of the Chemical Society, 1959 , p. 1310
反应条件
n-butyllithium 1) diethyl ether, hexane, -15 to -10 deg C, 25 min, -10 deg C, 10 min, rt, 45 min; 2) diethyl ether, hexane, rt, 30 min; Yield given. Multistep reaction;
参考文献
Guinot, Stephane G. R.; Hepworth, John D.; Wainwright, Mark
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 2 p. 297 - 303
