2-(beta-吗啉基乙基)吡啶合成路线 (共 5 条)
参考文献
Reich; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 4913
反应条件
1: 2 percent Chromat. / PPh3 / [Rh(cod)2]BF4 / tetrahydrofuran / 20 h / Heating
2: 2 percent Chromat. / Pd/C / tetrahydrofuran / 48 h / 760 Torr
View Scheme
参考文献
Beller, Matthias; Trauthwein, Harald; Eichberger, Martin; Breindl, Claudia; Mueller, Thomas E.
European Journal of Inorganic Chemistry, 1999 , # 7 p. 1121 - 1132
反应条件
triphenylphosphine; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in tetrahydrofuran
Alkylation; 20 h; Heating;
参考文献
Beller, Matthias; Trauthwein, Harald; Eichberger, Martin; Breindl, Claudia; Mueller, Thomas E.
European Journal of Inorganic Chemistry, 1999 , # 7 p. 1121 - 1132
反应条件
triethylaluminum; cobalt(II) 2-ethylhexanoate in toluene
T=150°C; 10 h; autoclave; Yield given. Yields of byproduct given;
参考文献
Selimov, F. A.; Khafizov, V. R.; Dzhemilev, U. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 3 p. 290 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 3 p. 360 - 365
反应条件
acetic acid
20 h; Heating;
参考文献
Ivanov, Ivo C.; Karagiosov, Stoyan K.; Sulay, Piroshka B.
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 181 - 182