in neat (no solvent) Ge-compound distilled into a vessel held at -196°C containing organic compound, mixture reacted at room temp. for 10 min; filtered in N2, volatiles removed in vac.;

in neat (no solvent) Ge-compound distilled into a vessel held at -196°C containing organic compound, mixture reacted at room temp. for 10 min; filtered in N2, volatiles removed in vac.;

water in neat (no solvent) condensation of excess of water onto Ge-compd. (-196°C), warming to room temp., standing for 60 min; fractional low-temp. distn. (collection of excess water at -23°C,of product at -196°C);

hydrogen sulfide in neat (no solvent) condensation of excess of H2S onto Ge-compd. (-196°C), warming toroom temp., standing for 60 min; fractional low-temp. distn. (collection at -196°C);

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '969212', constants.ctx, '0')">benzene</a> <br />&nbsp;excess of (CH3)3GeCl; at boiling temp. of the solvent;; distn.;;&nbsp;<br /> &nbsp;