1H-吲唑-3-基苯基甲酮合成路线 （共 15 条）
反应条件
1: copper (II) acetate monohydrate; oxygen / methanol / 90 °C / |Schlenk technique
2: ammonium cerium (IV) nitrate / methanol / 1 h
View Scheme
参考文献
Fang, Yan; Wang, Chengming; Su, Shengqin; Yu, Haizhu; Huang, Yong
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 7 p. 1061 - 1071
反应条件
1.1: 98 percent / dimethylaminopyridine; triethylamine / CH2Cl2 / 3 h / 0 - 20 °C
2.1: magnesium / diethyl ether / 1 h / Heating
2.2: 70 percent / diethyl ether / 0.17 h / Heating
View Scheme
参考文献
Crestey, Francois; Stiebing, Silvia; Legay, Remi; Collot, Valerie; Rault, Sylvain
Tetrahedron, 2007 , vol. 63, # 2 p. 419 - 428
反应条件
sulfuric acid; water
T=45°C; 10 h;
参考文献
Fedenok, Lidiya G.; Shvartsberg, Mark S.; Bashurova, Valentina S.; Bogdanchikov, George A.
Tetrahedron Letters, 2010 , vol. 51, # 1 p. 67 - 69
反应条件
n-butyllithium; tert.-butyl lithium
1a.) THF, -78 deg C, 5 min, 1b.) -78 deg C, 15 min, 2.) -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Welch; Hanau; Whalen
Synthesis, 1992 , # 10 p. 937 - 939
反应条件
diethyl ether
Behandeln des Reaktionsprodukts mit verd. Salzsaeure und mit Wasser;
参考文献
Meisenheimer; Diedrich
Chemische Berichte, 1924 , vol. 57, p. 1717
