(s)-(9ci)-alpha-(1-甲基乙基)-1H-苯并咪唑-2-甲胺合成路线 （共 6 条）
反应条件
trifluoroacetic acid in dichloromethane
3 h;
参考文献
Ghosh, Kumaresh; Sarkar, Tanmay
Supramolecular Chemistry, 2012 , vol. 24, # 10 p. 748 - 754,7
反应条件
hydrogenchloride in water
T=120°C; 72 h; Inert atmosphere;
参考文献
Li, Yuehui; Ding, Kuiling; Sandoval, Christian A.
Organic Letters, 2009 , vol. 11, # 4 p. 907 - 910
反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 19 h
2: acetic acid / 2 h / |Heating
3: trifluoroacetic acid / dichloromethane / 3 h
View Scheme
参考文献
Ghosh, Kumaresh; Sarkar, Tanmay
Supramolecular Chemistry, 2012 , vol. 24, # 10 p. 748 - 754,7
反应条件
1: acetic acid / 2 h / |Heating
2: trifluoroacetic acid / dichloromethane / 3 h
View Scheme
参考文献
Ghosh, Kumaresh; Sarkar, Tanmay
Supramolecular Chemistry, 2012 , vol. 24, # 10 p. 748 - 754,7
反应条件
1: dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 19 h
2: acetic acid / 2 h / |Heating
3: trifluoroacetic acid / dichloromethane / 3 h
View Scheme
参考文献
Ghosh, Kumaresh; Sarkar, Tanmay
Supramolecular Chemistry, 2012 , vol. 24, # 10 p. 748 - 754,7
反应条件
5-palladium/activated carbon; hydrogen in methanol
3 h;
参考文献
Zhang, Datong; Wang, Zongheng; Xu, Weiren; Sun, Fanggang; Tang, Lida; Wang, Jianwu
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 5 p. 2202 - 2210
