1: oleic acid chloride With pyridine in 1-methyl-pyrrolidin-2-one
T=20°C;
2: [Fluorescein]-Sphingosine in tetrahydrofuran
T=20°C; Further stages.;
参考文献
Chang, Young-Tae; Choi, Jaehwa; Ding, Sheng; Prieschl, Eva E.; Baumruker, Thomas; Lee, Jae-Mok; Chung, Sung-Kee; Schultz, Peter G.
Journal of the American Chemical Society, 2002 , vol. 124, # 9 p. 1856 - 1857
1: 1.) DIBAL-H / 2.) ether, toluene, warming from 5 to 23 deg C, 1 h
2: 1.27 g / 2 N HCl / tetrahydrofuran / 16 h / 25 °C
3: pyridine / 16 h / 25 °C
4: 92 percent / 1 N NaOH / methanol / 16 h / 25 °C
View Scheme
参考文献
Tkaczuk, Peter; Thornton, Edward R.
Journal of Organic Chemistry, 1981 , vol. 46, p. 4393 - 4398
