1,3-二(乙酰基氧基)-1,1,3,3-四丁基二锡氧烷合成路线 （共 9 条）
反应条件
in tetrahydrofuran; dichloromethane byproducts: (Bu4N)OSO2CH3; under N2, Schlenk setup, 1:1 mixt., Bu4N(CH3COO) soln. in THF added to suspn. of tin compd. in CH2Cl2 (1:1), stirred for 8-10 h at room temp.; concd., pptd. (Et2O), filtered, concd., dried (vac.), elem. anal.;
参考文献
Shankar, Ravi; Kumar, Mukesh; Chadha, Raj K.; Narula, Suraj P.
Polyhedron, 2004 , vol. 23, # 1 p. 71 - 75
反应条件
T=250°C; 0.5 h; Inert atmosphere; Product distribution / selectivity;
参考文献
EP2078724 A1, ;
Page/Page column 35 ;
反应条件
in not given partial hydrolysis; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 575, # 2 p. 286 - 300
反应条件
T=150°C; P=760.051 Torr; 5 h; Inert atmosphere;
参考文献
EP2226328 A1, ;
Page/Page column 65 ;
反应条件
T=140°C; P=760.051 Torr; 7 h; Inert atmosphere;
参考文献
EP2226328 A1, ;
Page/Page column 66 ;
反应条件
in hexane recrystn.; elem. anal.;
参考文献
Gross, David C.
Inorganic Chemistry, 1989 , vol. 28, p. 2355 - 2359
反应条件
T=140°C; P=760.051 Torr; 7 h; Inert atmosphere;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2226328 A1, 2010 ;
Location in patent: Page/Page column 66 ;
反应条件
T=150°C; P=760.051 Torr; 5 h; Inert atmosphere;
参考文献
EP2226328 A1, ;
Page/Page column 65 ;
反应条件
T=140°C; P=760.051 Torr; 7 h; Inert atmosphere;
参考文献
EP2226328 A1, ;
Page/Page column 66 ;
