反应条件
1: 2-methoxy-N,N-diethyl-benzamide With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran
T=-78°C; 0.5 h;
2: dimethyl-disulfide in tetrahydrofuran
T=-78 - 20°C; 4.25 h;
参考文献
Dittmann, Marc; Graupner, Franziska F.; Maerz, Benjamin; Oesterling, Sven; Devivie-Riedle, Regina; Zinth, Wolfgang; Engelhard, Martin; Luettke, Wolfgang
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 591 - 594
Angew. Chem., 2013 , vol. 126, # 2 p. 602 - 605,4
