2,2-二甲基-3-氧代丁酸乙酯合成路线 (共 56 条)
反应条件
tetrabutylammomium bromide in dichloromethane T=20°C; diaphragm cell, platinum cathode; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 6.2 p. 1332
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1451
反应条件
sodium hydride; N,N-dimethyl-formamide; benzene anschliessend mit Methyljodid;
参考文献
Journal of Organic Chemistry, , vol. 21, p. 245
反应条件
tetra-n-butylammonium tetrafluoroborate; zinc dibromide; zinc in acetonitrile Ambient temperature;
参考文献
Rollin, Y.; Gebehenne, C.; Derien, S.; Dunach, E.; Perichon, J.
Journal of Organometallic Chemistry, 1993 , vol. 461, # 1-2 p. 9 - 14
反应条件
1,1,1,2,2,2-hexabutyl-distannane in cyclohexane 36 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1139 - 1144
反应条件
mercury dichloride; zinc in diethyl ether; benzene
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 11, p. 2360 - 2362
Zhurnal Organicheskoi Khimii, , vol. 11, # 11 p. 2319 - 2322
参考文献
Tetrahedron, , vol. 27, p. 4777 - 4785
参考文献
Chemische Berichte, , vol. 55, p. 3346
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 41, # 10 p. 740 - 744
反应条件
1: 1.) LDA / 1.) THF, -75 deg C, 30 min, 2.) -75 deg C, 2 h 2: 180 - 190 °C View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 41, # 10 p. 740 - 744
参考文献
Gazzetta Chimica Italiana, , vol. 93, p. 451 - 454