2-乙基-2-硝基-1,3-丙二醇合成路线 (共 16 条)
反应条件
PPA; copper P=3 - 6 Torr; (heating);
参考文献
Kissinger,L.W. et al.
Tetrahedron, Supplement, 1964 , vol. 6, p. 317 - 323
参考文献
Vanderbilt; Hass
Industrial and Engineering Chemistry, 1940 , vol. 32, p. 35
Full Text Show Details
Johnson; Degering
Journal of Organic Chemistry, 1943 , vol. 8, p. 11
反应条件
5 palladium on charcoal; hydrogen in methanol T=100°C; P=3102.97 Torr; 10 h; Reagent/catalystTemperature;
参考文献
ANGUS CHEMICAL COMPANY; MOORE, David, W.; GREEN, George, D.
Patent: WO2013/133925 A1, 2013 ;
Location in patent: Paragraph 0019; 0021; 0022; 0023; 0024 ;
反应条件
methanol; nickel T=50°C; P=51485.6 Torr; Hydrogenation;
参考文献
Industrial and Engineering Chemistry, , vol. 32, p. 35
Journal of Organic Chemistry, , vol. 8, p. 11
参考文献
Vanderbilt; Hass
Industrial and Engineering Chemistry, 1940 , vol. 32, p. 35
Full Text Show Details
Johnson; Degering
Journal of Organic Chemistry, 1943 , vol. 8, p. 11
参考文献
Vanderbilt; Hass
Industrial and Engineering Chemistry, 1940 , vol. 32, p. 35
Full Text Show Details
Purdue Research Found.
Patent: US2139120 , 1937 ;
Full Text Show Details
Purdue Research Found.
Patent: US2132330 , 1937 ;
Full Text Show Details
Purdue Research Found.
Patent: US2135444 , 1937 ;
反应条件
in water
T=40°C; 2 h; Product distribution / selectivity;
参考文献
Moore, David W.
Patent: US2011/224460 A1, 2011 ;
Location in patent: Page/Page column 3-4; 5 ;
参考文献
Pauwels
Chem. Zentralbl., 1898 , vol. 69, # I p. 193
参考文献
Piloty; Ruff
Chemische Berichte, 1898 , vol. 31, p. 225