4-乙氧基-3-硝基苯甲酸合成路线 (共 17 条)
反应条件
sodium hydroxide in tetrahydrofuran; ethanol; water T=20°C; 72 h;
参考文献
TAKEDA CHEMICAL INDUSTRIES, LTD.
Patent: WO2004/46107 A1, 2004 ;
Location in patent: Page 92-93 ;
WO 2004/046107 A1
反应条件
1: sodium ethanolate / ethanol; water 2: sodium hydroxide / dichloromethane; ethanol View Scheme
参考文献
US2012/129843 A1, ;
US2012/129842 A1, ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / |Inert atmosphere 2: potassium hydroxide; water / 1.2 h / |Reflux View Scheme
反应条件
1: sulfuric acid 2: nitric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 127, p. 2649
参考文献
Journal of the Chemical Society, , vol. 127, p. 2649
反应条件
permanganate(VII) ion
参考文献
Chemische Berichte, , vol. 59, p. 906
反应条件
potassium permanganate; acetic acid
参考文献
Journal of the Chemical Society, , p. 203,205
反应条件
1: sulfuric acid 2: nitric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 127, p. 2649
反应条件
1: glacial acetic acid 2: sodium ethylate 3: permanganate View Scheme
参考文献
Chemische Berichte, , vol. 59, p. 906
反应条件
1: glacial acetic acid; hydrobromic acid 2: glacial acetic acid 3: sodium ethylate 4: permanganate View Scheme
参考文献
Chemische Berichte, , vol. 59, p. 906