4-叔丁基-3-硝基苯甲酸合成路线 (共 9 条)
反应条件
1: (i) (decarboxylation), (ii) (nitration) 2: aq. Na2S2 3: (i) NaNO2, aq. HCl, (ii) H3PO2 View Scheme
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618
反应条件
1: (i) (decarboxylation), (ii) (nitration) 2: aq. Na2S2 3: (i) NaNO2, aq. HCl, (ii) H3PO2 4: Fe, H2O / acetic acid View Scheme
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618
反应条件
1: (i) (decarboxylation), (ii) (nitration) 2: aq. Na2S2 View Scheme
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618
反应条件
potassium hydroxide; potassium permanganate
参考文献
Skinner; Zell
Journal of the American Chemical Society, 1955 , vol. 77, p. 5441
反应条件
1: concentrated aqueous sulfuric acid; nitric acid
2: aqueous KOH; KMnO4
View Scheme
参考文献
Skinner; Zell
Journal of the American Chemical Society, 1955 , vol. 77, p. 5441
参考文献
Doepp,D.; Brugger,E.
Liebigs Annalen der Chemie, 1979 , p. 554 - 563
反应条件
1: (i) 1-methyl-pyrrolidin-2-one, (ii) FeCl3, aq. HCl
2: aq. H2SO4
View Scheme
参考文献
Doepp,D.; Brugger,E.
Liebigs Annalen der Chemie, 1979 , p. 554 - 563
反应条件
sulfuric acid; nitric acid
参考文献
Bell
Journal of the Chemical Society, 1956 , p. 3243
反应条件
(i) (decarboxylation), (ii) (nitration); Multistep reaction;
参考文献
Lesslie,M.S.; Mayer,U.J.H.
Journal of the Chemical Society, 1961 , p. 611 - 618