1: With copper(l) iodide in DMF (N,N-dimethyl-formamide) T=145 - 150°C; 28 h; 2: With ethylenediamine in DMF (N,N-dimethyl-formamide); water T=25 - 30°C; 2 h;
1: With pyridine; thionyl chloride T=20 - 25°C; 1 h; 2: With trichlorophosphate 4 h;
参考文献
Greenwood, Alan Kenneth; McHattie, Derek; Rechka, Josef A.; Hedger, Paul C.M.; Gamble, Mark P.
Patent: US2004/14997 A1, 2004 ;
Location in patent: Page 12 ;
trichlorophosphate in acetonitrile T=60°C; Heating / reflux;
参考文献
Greenwood, Alan Kenneth; McHattie, Derek; Rechka, Josef A.; Hedger, Paul C.M.; Gamble, Mark P.
Patent: US2004/14997 A1, 2004 ;
Location in patent: Page 11 ;
