4-(戊氧基)-4’-联苯羧酸合成路线 （共 11 条）
反应条件
1: With potassium hydroxide in ethanol; water 24 h; Inert atmosphereReflux; 2: With hydrogenchloride in ethanol; water pH=6;
参考文献
Yao, Jianzhong; Liu, Hongming; Zhou, Ting; Chen, Hai; Miao, Zhenyuan; Dong, Guoqiang; Wang, Shengzheng; Sheng, Chunquan; Zhang, Wannian
Tetrahedron, 2012 , vol. 68, # 14 p. 3074 - 3085
反应条件
sodium bromide; zirconium monoxide; manganese; cobalt in acetic anhydride; acetic acid T=105°C; Oxidation;
参考文献
Brilev, V. V.; Vasilevskii, D. A.; Tarasevich, V. A.; Matveenko, Yu. V.; Erdman, A. A.
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, 1999 , vol. 69, # 1 p. 126 - 129
反应条件
potassium hydroxide in methanol; water 120 h; Heating;
参考文献
Goodby; Pindak
Molecular crystals and liquid crystals, 1981 , vol. 75, # 1-4 p. 233 - 247
反应条件
2: 77 percent / NaBr / Co-Mn-ZrO / acetic acid; acetic anhydride / 105 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, , vol. 69, # 1 p. 126 - 129
反应条件
2: 77 percent / NaBr / Co-Mn-ZrO / acetic acid; acetic anhydride / 105 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, , vol. 69, # 1 p. 126 - 129
反应条件
1: Pd/C / 270 - 310 °C 3: 77 percent / NaBr / Co-Mn-ZrO / acetic acid; acetic anhydride / 105 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, , vol. 69, # 1 p. 126 - 129
反应条件
1: 1.) sodium hydroxide / 1.) dioxan, water, reflux, 3 h; 2.) reflux, 2 h 2: 48 percent / various solvent(s) / 3 h / Heating 3: 76 percent / potassium hydroxide / H2O; methanol / 120 h / Heating View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 75, # 1-4 p. 233 - 247
反应条件
1: 48 percent / various solvent(s) / 3 h / Heating 2: 76 percent / potassium hydroxide / H2O; methanol / 120 h / Heating View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 75, # 1-4 p. 233 - 247
反应条件
1: 1.) sodium hydroxide / 1.) dioxan, water, reflux, 3 h; 2.) reflux, 2 h 2: 48 percent / various solvent(s) / 3 h / Heating 3: 76 percent / potassium hydroxide / H2O; methanol / 120 h / Heating View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 75, # 1-4 p. 233 - 247
参考文献
Journal of the Chemical Society, , p. 1412,1414, 1418, 1420
