4-正辛氧基联苯-4-甲酸合成路线 （共 15 条）
反应条件
1: With potassium hydroxide in ethanol; water 24 h; Inert atmosphereReflux; 2: With hydrogenchloride in ethanol; water pH=6;
参考文献
Yao, Jianzhong; Liu, Hongming; Zhou, Ting; Chen, Hai; Miao, Zhenyuan; Dong, Guoqiang; Wang, Shengzheng; Sheng, Chunquan; Zhang, Wannian
Tetrahedron, 2012 , vol. 68, # 14 p. 3074 - 3085
反应条件
sodium hydroxide in ethylene glycol
参考文献
FR2288732DE2450088 , ;
Chem.Abstr., , vol. 85, # 46219
反应条件
1: With water; potassium hydroxide in ethanol 26 h; Reflux; 2: With hydrogenchloride in ethanol; water T=20°C;
参考文献
Mori, Takeshi; Kijima, Masashi
Molecular Crystals and Liquid Crystals, 2008 , vol. 489, p. 246/[572]-256/[582]
反应条件
hydrogenchloride; sodium hydroxide in water; dimethyl sulfoxide
反应条件
1.1: 97 percent / sulfuric acid / 6 h / Heating 2.1: potassium carbonate / butan-2-one / 6 h / Heating 2.2: aq. potassium hydroxide / ethanol; H2O / 0.5 h / Heating 2.3: 74 percent / aq. HCl / H2O / 3 h / Heating View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 414, p. 27 - 38
反应条件
1: K2CO3 / dimethylformamide 2: NaOH / ethanol View Scheme
参考文献
Molecules, , vol. 5, # 3 p. 383 - 385
反应条件
1: With potassium carbonate in butanone 6 h; Heating; 2: With potassium hydroxide in ethanol; water 0.5 h; Heating; 3: With hydrogenchloride in water 3 h; Heating;
参考文献
Tokushige; Mihara; Koide
Molecular Crystals and Liquid Crystals, 2004 , vol. 414, p. 27 - 38
反应条件
1: 45 percent / potassium tert-butoxide / acetonitrile / 17 h / Heating 2: 2 N aq. NaOH / dioxane / 17 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 17 p. 3271 - 3281
反应条件
sodium hydroxide in methanol Hydrolysis; Heating;
参考文献
Journal of Materials Chemistry, , vol. 10, # 6 p. 1297 - 1302
反应条件
1: K2CO3 / acetone / Heating 2: aq. NaOH / methanol / Heating View Scheme
参考文献
Journal of Materials Chemistry, , vol. 10, # 6 p. 1297 - 1302
