N-(3- 醛基苯基)乙酰胺合成路线 （共 15 条）
反应条件
1: iron; ammonium chloride / water; ethanol / |Inert atmosphere; |Reflux
2: triethylamine / dichloromethane / 16 h / 20 °C / |Inert atmosphere
3: sodium hydroxide / methanol / 2.5 h / 20 °C / |Inert atmosphere
4: Dess-Martin periodane / dichloromethane / 0.33 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Storz, Michael P.; Maurer, Christine K.; Zimmer, Christina; Wagner, Nathalie; Brengel, Christian; De Jong, Johannes C.; Lucas, Simon; Muesken, Mathias; Haeussler, Susanne; Steinbach, Anke; Hartmann, Rolf W.
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16143 - 16146
反应条件
1: sodium hydroxide / methanol / 2.5 h / 20 °C / |Inert atmosphere
2: Dess-Martin periodane / dichloromethane / 0.33 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Storz, Michael P.; Maurer, Christine K.; Zimmer, Christina; Wagner, Nathalie; Brengel, Christian; De Jong, Johannes C.; Lucas, Simon; Muesken, Mathias; Haeussler, Susanne; Steinbach, Anke; Hartmann, Rolf W.
Journal of the American Chemical Society, 2012 , vol. 134, # 39 p. 16143 - 16146
反应条件
N-bromoacetamide in water
T=14.9 - 34.9°C; ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Banerji, Kalyan K.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3717 - 3722
参考文献
Friedlaender; Fritsch
Monatshefte fuer Chemie, 1903 , vol. 24, p. 8
反应条件
Behandlung des (amorphen) Reaktionsprodukts mit Acetanhydrid.Hydrogenation;
参考文献
Rupe; Vogler
Helvetica Chimica Acta, 1925 , vol. 8, p. 834
