1-(4-氯苯基)-1-苯基乙醇合成路线 (共 25 条)
反应条件
in diethyl ether
T=0°C;
参考文献
Maclin, Keith M.; Richey Jr., Herman G.
Journal of Organic Chemistry, 2002 , vol. 67, # 12 p. 4370 - 4371
反应条件
in diethyl ether
20 h; -20 deg C to r.t.;
参考文献
Dimitrov; Stanchev; Milenkov; Nikiforov; Demirev
Synthesis, 1991 , # 3 p. 228 - 232
反应条件
in diethyl ether
T=0°C; competition reaction with bezophenone and 4-chlorobenzophenone, relative velocity constant;
参考文献
Yamataka, Hiroshi; Fujimura, Naoya; Kawafuji, Yukie; Hanafusa, Terukiyo
Journal of the American Chemical Society, 1987 , vol. 109, # 14 p. 4305 - 4308
反应条件
1: 1.) anhydr. manganese bromide / 1.) 0 deg C then 20 deg C, 45 min; 2.) 0 deg C then 20 deg C, 1.5 h
2: 0 deg C then 20 deg C, 4h
View Scheme
参考文献
Cahiez, Gerard; Rivas-Enterrios, Jose; Clery, Patrick
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3659 - 3662
反应条件
1: 1.) anhydr. manganese bromide / 1.) 0 deg C then 20 deg C, 45 min; 2.) 0 deg C then 20 deg C, 1.5 h
2: 0 deg C then 20 deg C, 4h
View Scheme
参考文献
Cahiez, Gerard; Rivas-Enterrios, Jose; Clery, Patrick
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3659 - 3662
反应条件
1H-imidazole; water; dihydrogen peroxide; MnTPFPS4PCl in methanol; dichloromethane
T=20°C; 24 h; also without water, var. catalyst; Product distribution;
参考文献
Froehlich; Pietzyk; Smolinka; Goeber
Pharmazie, 1996 , vol. 51, # 6 p. 409 - 414
参考文献
Asta-Werke
Patent: DE952715 , 1952 ;
反应条件
0 deg C then 20 deg C, 4h; Yield given;
参考文献
Cahiez, Gerard; Rivas-Enterrios, Jose; Clery, Patrick
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3659 - 3662
参考文献
Novak; Protiva
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 3966,3974
反应条件
1.) 0 to 20 deg C, 1.5 h; 2.) 0 to 20 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Cahiez, Gerard; Rivas-Enterrios, Jose; Clery, Patrick
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3659 - 3662