3-甲基-1,2-丁二烯合成路线 (共 178 条)
参考文献
Cripps et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2723,2725
反应条件
in benzene Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Pasto, Daniel J.; Cottard, Francois
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4642 - 4646
反应条件
1: quinoline hydrobromide; quinoline / 130 - 135 °C 2: hydrobromic acid View Scheme
参考文献
Kutscherow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1913 , vol. 45, p. 1653
Chem. Zentralbl., 1914 , vol. 85, # I p. 754
反应条件
hydrogenchloride; oxygen; copper dichloride; palladium dichloride T=0 - 25°C; P=760 Torr;
参考文献
Alper, Howard; Hartstock, Frederick W.; Despeyroux, Bertrand
Journal of the Chemical Society, Chemical Communications, 1984 , # 14 p. 905 - 906
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; caesium carbonate in 1,2-dichloro-ethane T=60°C; 24 h;
参考文献
In, Su Kim; Krische, Michael J.
Organic Letters, 2008 , vol. 10, # 3 p. 513 - 515
反应条件
C21H38AuClNP*C24BF20(1-)*K(1+) in benzene-d6 T=90°C; Markovnikov hydroamination; 12 h; Inert atmosphere;
参考文献
Xiaoming, Zeng; Soleilhavoup, Michele; Bertrand, Guy
Organic Letters, 2009 , vol. 11, # 15 p. 3166 - 3169
反应条件
bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in toluene T=50°C; Addition; hydroboration; 2 h;
参考文献
Yamamoto, Yasunori; Fujikawa, Ryou; Yamada, Akihiko; Miyaura, Norio
Chemistry Letters, 1999 , # 10 p. 1069 - 1070
反应条件
CF3O3S(1-)*C30H33NPPd(1+) in benzene-d6 T=25°C; 3 h; Inert atmosphere;
参考文献
Kuchenbeiser, Glenn; Shaffer, Andrew R.; Zingales, Nicholas C.; Beck, John F.; Schmidt, Joseph A.R.
Journal of Organometallic Chemistry, 2011 , vol. 696, # 1 p. 179 - 187
反应条件
lithium perchlorate in methanol electrochemical oxidation, 1.64 V; Title compound not separated from byproducts;
参考文献
Becker, James Y.; Zinger, Baruch
Tetrahedron, 1982 , vol. 38, # 11 p. 1677 - 1682
反应条件
lithium perchlorate in methanol electrochemical oxidation, 1.84 V; Mechanism;
参考文献
Becker, James Y.; Zinger, Baruch
Tetrahedron, 1982 , vol. 38, # 11 p. 1677 - 1682