copper(l) iodide; boron trifluoride diethyl etherate
other ratio of reagents; Product distribution;
参考文献
Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide; water
T=20°C; Heck reaction; 0.25 h;
2: bromobenzene With palladium diacetate in N,N-dimethyl acetamide; water
T=120°C; Heck reaction; 6 h; Further stages. Title compound not separated from byproducts.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine; tetrabutylammomium bromide in N,N-dimethyl acetamide; water
T=20°C; Heck reaction; 0.25 h;
2: bromobenzene With 4'-hydroxyacetophenone oxime palladacycle catalyst in N,N-dimethyl acetamide; water
T=120°C; Heck reaction; 6 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
1: 3-hydroxy-1-butene With α-cyclohexylcyclohexanemethanamine in water
T=20°C; Heck reaction; 0.25 h;
2: iodobenzene With Kaiser oxime-derived complex on resin base in water
T=120°C; Heck reaction; 6 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
