1,2-二氯-1,2-二氟乙烯合成路线 (共 109 条)
反应条件
in monofluoro-trichloromethane
T=-105°C; competition with ClFC=CFCl and H2C=CF2, relative addition rates and orientation ratios; Rate constantProduct distribution;
参考文献
Navarrini, W.; Russo, A.; Tortelli, V.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6441 - 6443
反应条件
in monofluoro-trichloromethane
T=-105°C; competition with ClFC=CFCl and H2C=CHF, relative addition rates and orientation ratios; Rate constantProduct distribution;
参考文献
Navarrini, W.; Russo, A.; Tortelli, V.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6441 - 6443
反应条件
in monofluoro-trichloromethane
T=-105°C; competition with ClFC=CFCl and H2C=CHF, relative addition rates and orientation ratios; Rate constantProduct distribution;
参考文献
Navarrini, W.; Russo, A.; Tortelli, V.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6441 - 6443
反应条件
fluorine
T=-80°C; 4 h;
参考文献
Solvay Solexis S.p.A.
Patent: EP1388531 A1, 2004 ;
Location in patent: Page column 9 ;
反应条件
fluorine
T=-80°C; 4 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/30146 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
1: 1,1,2,2-tetrafluoroethylene; Difluoromethylene bishypofluorite T=-114°C; 6.6 h;
2: 1,2-difluoro-1,2-dichloroethylene T=-70°C;
参考文献
Navarrini, Walter; Corti, Sandra
Journal of Fluorine Chemistry, 2004 , vol. 125, # 2 p. 189 - 197
反应条件
in monofluoro-trichloromethane
T=-78°C; competition with ClFC=CClF and Cl2C=CHCl, relative addition rates and orientation ratios; Rate constantProduct distribution;
参考文献
Navarrini, W.; Russo, A.; Tortelli, V.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6441 - 6443
反应条件
aluminium trichloride
参考文献
Paleta,O. et al.
Collection of Czechoslovak Chemical Communications, 1967 , vol. 32, p. 3888 - 3896
反应条件
n-butyllithium in tetrahydrofuran; diethyl ether; hexane
T=-70 - -65°C; 1 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 1.2, page 1 - 15