1,2-二氯-1,2-二氟乙烯合成路线 (共 109 条)
反应条件
disulfur dichloride; sulfur(IV) fluoride; hydrogen fluoride T=60°C; 1 h; stainless-steel autoclave; Yield given;
参考文献
Muratov, N. N.; Mohamed, Nagib Muhbar; Kushenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 5 p. 862 - 866
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 964 - 969
反应条件
disulfur dichloride; sulfur(IV) fluoride; hydrogen fluoride T=60°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Muratov, N. N.; Mohamed, Nagib Muhbar; Kushenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 5 p. 862 - 866
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 964 - 969
反应条件
T=900°C; 0.00105556 h; other temperature, other contact time; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 59, # 3.2 p. 622 - 630,551 - 558
反应条件
T=600°C; 0.00105556 h; other temperature, other contact time; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 59, # 3.2 p. 622 - 630,551 - 558
参考文献
SOLVAY SOLEXIS S.P.A.
Patent: WO2009/87067 A1, 2009 ;
Location in patent: Page/Page column 12-13 ;
反应条件
fluorine; cesium fluoride in CF2ClCF3 T=-80°C; 3 h;
参考文献
Solvay Solexis S.p.A.
Patent: EP1457484 A1, 2004 ;
Location in patent: Page column 6-7 ;
反应条件
fluorine in 1,1,1,2,2-pentafluoro-2-chlorethyl T=-80°C; 3 h;
参考文献
SOLVAY SOLEXIS S.p.A.
Patent: US2004/199009 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
fluorine T=-80°C; 4 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/30146 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
fluorine T=-100°C; 2 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/30146 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
fluorine T=-100 - -80°C; 6.5 h;
参考文献
Solvay Solexis S.p.A.
Patent: US2004/30146 A1, 2004 ;
Location in patent: Page 3 ;