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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
59826-16-3
合成路线
（共 8 条）
→
反应条件
59826-16-3
反应条件
potassium carbonate in acetone
参考文献
American Home Products Corporation
Patent: US2002/28832 A1, 2002 ;
US 20020028832 A1
59430-56-7
→
反应条件
59826-16-3
反应条件
potassium carbonate in water; acetone 4 h; Heating;
参考文献
Tominaga; Tone; Nakagawa; Takada; Hoshino; Watanabe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 8 p. 2166 - 2181
59430-56-7
+
100-39-0
溴化苄
→
反应条件
59826-16-3
反应条件
potassium carbonate in water; acetone
参考文献
Steffan, Robert J.; Ashwell, Mark A.; Solvibile, William R.; Matelan, Edward; Largis, Elwood; Han, Stella; Tillet, Jeffery; Mulvey, Ruth
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 20 p. 2957 - 2961
79784-30-8
→
反应条件
59826-16-3
反应条件
1: 47 percent / H2 / Raney Ni / propan-2-ol; tetrahydrofuran 2: 80 percent / 48 percent HBr / Heating 3: 27 percent / K2CO3 / acetone; H2O View Scheme
参考文献
Ashwell, Mark A; Solvibile Jr., William R; Han, Stella; Largis, Elwood; Mulvey, Ruth; Tillet, Jeffrey
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 24 p. 3123 - 3127
102-56-7
2,5-二甲氧基苯胺
→
反应条件
59826-16-3
反应条件
1: 99 percent / Et3N / benzene 2: 78 percent / HCl 3: 47 percent / H2 / Raney Ni / propan-2-ol; tetrahydrofuran 4: 80 percent / 48 percent HBr / Heating 5: 27 percent / K2CO3 / acetone; H2O View Scheme
参考文献
Ashwell, Mark A; Solvibile Jr., William R; Han, Stella; Largis, Elwood; Mulvey, Ruth; Tillet, Jeffrey
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 24 p. 3123 - 3127
79784-29-5
→
反应条件
59826-16-3
反应条件
1: 78 percent / HCl 2: 47 percent / H2 / Raney Ni / propan-2-ol; tetrahydrofuran 3: 80 percent / 48 percent HBr / Heating 4: 27 percent / K2CO3 / acetone; H2O View Scheme
参考文献
Ashwell, Mark A; Solvibile Jr., William R; Han, Stella; Largis, Elwood; Mulvey, Ruth; Tillet, Jeffrey
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 24 p. 3123 - 3127
61306-74-9
→
反应条件
59826-16-3
反应条件
1: 80 percent / 40 percent aq. HBr 2: 27 percent / K2CO3 / acetone View Scheme
参考文献
Steffan, Robert J.; Ashwell, Mark A.; Solvibile, William R.; Matelan, Edward; Largis, Elwood; Han, Stella; Tillet, Jeffery; Mulvey, Ruth
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 20 p. 2957 - 2961
59826-16-3
→
反应条件
65008-41-5
反应条件
1: 56 percent / K2CO3 / propan-2-ol / 5 h / 70 - 80 °C 2: 43.6 percent / methanol / 20 h / Ambient temperature 3: 77.2 percent / hydrogen / 10percent Pd-C / methanol; H2O / 8 h / Ambient temperature View Scheme
参考文献
Tominaga; Tone; Nakagawa; Takada; Hoshino; Watanabe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 8 p. 2166 - 2181
